Stoe Image plate diffraction system-2T diffractometer | 1688 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.016 |
φ oscillation scans | θmax = 29.4°, θmin = 4.6° |
Absorption correction: numerical [X-RED (Stoe & Cie, 2001) and X-SHAPE (Stoe & Cie, 1999)] | h = −15→18 |
Tmin = 0.310, Tmax = 0.399 | k = −5→6 |
3251 measured reflections | l = −15→13 |
1696 independent reflections |