Bruker Kappa APEXII CCD area detector diffractometer | Rint = 0.031 |
phi and ω scans | θmax = 28.1°, θmin = 2.8° |
23620 measured reflections | h = −15→16 |
5984 independent reflections | k = −12→11 |
4634 reflections with I > 2σ(I) | l = −29→29 |
Bruker Kappa APEXII CCD area detector diffractometer | Rint = 0.031 |
phi and ω scans | θmax = 28.1°, θmin = 2.8° |
23620 measured reflections | h = −15→16 |
5984 independent reflections | k = −12→11 |
4634 reflections with I > 2σ(I) | l = −29→29 |