Table 4.
Detection results of the 37 suspected amatoxin poisonings in urine submitted for toxicological analysis including sample ID, sampling time after assumed ingestion, results of the affinity column chromatography and former developed methods5,6; h, hours; +, positive for α-, β-, and/or γ-amanitin; −, negative for α,-β-, and/or γ-amanitin; n.g., not given.
| Sample ID | Sampling time after assumed ingestion (h) | Detection result using immunoprecipitation | Detection result using solid-phase extraction5,6 |
|---|---|---|---|
| 1 | n.g | − | − |
| 2 | 18 | − | − |
| 3 | n.g | − | − |
| 4 | n.g | − | − |
| 5 | 30 | − | − |
| 6 | 28 | − | − |
| 7 | n.g | − | − |
| 8 | n.g | + | + |
| 9 | 11 | − | − |
| 10 | n.g | − | − |
| 11 | n.g | − | − |
| 12 | n.g | + | + |
| 13 | 144 | − | − |
| 14 | n.g | − | − |
| 15 | 192 | − | − |
| 16 | n.g | − | − |
| 17 | n.g | − | − |
| 18 | 43 | − | − |
| 19 | > 14 | − | − |
| 20 | n.g | − | − |
| 21 | n.g | − | − |
| 22 | 25 | − | − |
| 23 | 25 | − | − |
| 24 | n.g | − | − |
| 25 | n.g | − | − |
| 26 | 49 | + | + |
| 27 | n.g | + | + |
| 28 | n.g | − | − |
| 29 | 26 | − | − |
| 30 | n.g | + | + |
| 31 | n.g | + | + |
| 32 | n.g | + | + |
| 33 | 14 | + | + |
| 34 | 59 | − | − |
| 35 | 6 | − | − |
| 36 | n.g | − | − |
| 37 | n.g | − | − |