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. 2024 Jul 9;4(9):3501–3518. doi: 10.1021/jacsau.4c00398

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© 2024 The Authors. Published by American Chemical Society

Permits the broadest form of re-use including for commercial purposes, provided that author attribution and integrity are maintained (https://creativecommons.org/licenses/by/4.0/).

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Heat released upon C₄H₈O adsorption in (a) CH₃CN and (b) CH₃OH as a function of C₄H₈O to metal ratio over hydrophilic (solid) and hydrophilic (hollow) Al- (black) and Zr-BEA (blue) materials (0.005 M C₄H₈O, 308 K). Transparent points are omitted from the adsorption enthalpy calculation, denoted by the dashed line. Section S11 includes adsorption enthalpy calculation details, raw data for the ITC experiments from Figure 6, and further ITC measurements, including CH₃OH adsorption over each M-BEA.