Table 2. 13C NMR (125 MHz) Data for Compounds 1–7 in CDCl3.
|
δC,type |
|||||||
|---|---|---|---|---|---|---|---|
| No. | 1 | 2 | 3 | 4 | 5 | 6 | 7 |
| 1 | 34.8, CH2 | 34.8, CH2 | 34.8, CH2 | 34.8, CH2 | 34.1, CH2 | 33.8, CH2 | 33.8, CH2 |
| 2 | 27.6, CH2 | 27.7, CH2 | 27.6, CH2 | 27.6, CH2 | 27.5, CH2 | 27.6, CH2 | 27.5, CH2 |
| 3 | 78.3, CH | 78.3, CH | 78.3, CH | 78.2, CH | 78.4, CH | 78.4, CH | 78.4, CH |
| 4 | 38.8, C | 39.0, C | 39.0, C | 39.0, C | 39.2, C | 39.2, C | 39.2, C |
| 5 | 48.5, CH | 48.5, CH | 48.5, CH | 48.4, CH | 49.4, CH | 49.4, CH | 49.4, CH |
| 6 | 36.0, CH2 | 35.8, CH2 | 35.9, CH2 | 35.9, CH2 | 36.0, CH2 | 36.0, CH2 | 36.0, CH2 |
| 7 | 198.2, C | 198.3, C | 198.3, C | 198.4, C | 199.7, C | 200.2, C | 200.1, C |
| 8 | 139.1, C | 139.1, C | 139.1, C | 139.1, C | 143.5, C | 140.5, C | 140.5, C |
| 9 | 165.2, C | 165.4, C | 165.4, C | 165.5, C | 157.3, C | 161.3, C | 161.1, C |
| 10 | 39.5, C | 39.5, C | 39.5, C | 39.4, C | 38.4, C | 39.7, C | 39.7, C |
| 11 | 23.8, CH2 | 23.9, CH2 | 23.8, CH2 | 23.8, CH2 | 81.1, CH | 68.2, CH | 68.2, CH |
| 12 | 30.3, CH2 | 30.2, CH2 | 30.1, CH2 | 30.0, CH2 | 38.2, CH2 | 43.0, CH2 | 43.1, CH2 |
| 13 | 44.9, C | 44.9, C | 44.8, C | 44.8, C | 46.4, C | 46.4, C | 46.3, C |
| 14 | 47.9, C | 47.9, C | 47.8, C | 47.8, C | 48.0, C | 48.1, C | 48.2, C |
| 15 | 31.6, CH2 | 31.6, CH2 | 31.6, CH2 | 31.6, CH2 | 32.0, CH2 | 31.9, CH2 | 31.9, CH2 |
| 16 | 28.5, CH2 | 28.8, CH2 | 28.8, CH2 | 28.7, CH2 | 27.6, CH2 | 27.7, CH2 | 28.0, CH2 |
| 17 | 48.4, CH | 48.6, CH | 48.9, CH | 48.8, CH | 48.3, CH | 48.6, CH | 48.9, CH |
| 18 | 16.1, CH3 | 15.9, CH3 | 15.7, CH3 | 15.7, CH3 | 17.1, CH3 | 16.6, CH3 | 16.5, CH3 |
| 19 | 18.8, CH3 | 18.8, CH3 | 18.8, CH3 | 18.8, CH3 | 19.2, CH3 | 19.9, CH3 | 19.9, CH3 |
| 20 | 36.0, CH | 35.7, CH | 36.4, CH | 36.4, CH | 35.5, CH | 35.9, CH | 35.8, CH |
| 21 | 19.3, CH3 | 19.0, CH3 | 18.9, CH3 | 19.0, CH3 | 19.6, CH3 | 19.3, CH3 | 18.8, CH3 |
| 22 | 38.8, CH2 | 30.1, CH2 | 36.0, CH2 | 31.8, CH2 | 38.1, CH2 | 38.6, CH2 | 34.6, CH2 |
| 23 | 130.6, CH | 37.4, CH2 | 20.9, CH2 | 32.1, CH2 | 129.2, CH | 130.1, CH | 26.2, CH2 |
| 24 | 134.9, CH | 215.3, CH2 | 44.4, CH2 | 76.5, CH | 135.8, CH | 135.1, CH | 155.0, CH |
| 25 | 82.4, C | 41.1, CH | 209.2, C | 147.6, C | 82.5, C | 82.4, C | 139.9, C |
| 26 | 24.6, CH3 | 18.8, CH3 | 30.0, CH3 | 111.6, CH2 | 24.9, CH3 | 24.5, CH3 | 195.4, CH |
| 27 | 24.6, CH3 | 18.8, CH3 | – | 17.3, CH3 | 23.8, CH3 | 24.5, CH3 | 9.4, CH3 |
| 28 | 27.5, CH3 | 27.3, CH3 | 27.5, CH3 | 24.5, CH3 | 27.8, CH3 | 27.7, CH3 | 27.7, CH3 |
| 29 | 15.2, CH3 | 15.2, CH3 | 15.2, CH3 | 15.2, CH3 | 15.4, CH3 | 15.3, CH3 | 15.3, CH3 |
| 30 | 24.6, CH3 | 24.3, CH3 | 24.5, CH3 | 27.4, CH3 | 25.3, CH3 | 25.9, CH3 | 25.9, CH3 |