Table 4. 13C NMR (125 MHz) Data for Compounds 8–10 in CDCl3.
|
δC,type |
|||
|---|---|---|---|
| No. | 8 | 9 | 10 |
| 1 | 33.9, CH2 | 34.0, CH2 | 33.9, CH2 |
| 2 | 28.0, CH2 | 28.0, CH2 | 28.0, CH2 |
| 3 | 78.8, CH | 78.8, CH | 78.8, CH |
| 4 | 38.5, C | 38.6, C | 38.6, C |
| 5 | 45.5, CH | 45.6, CH | 45.6, CH |
| 6 | 28.6, CH2 | 28.6, CH2 | 28.6, CH2 |
| 7 | 65.6, CH | 65.6, CH | 65.6, CH |
| 8 | 157.3, C | 157.2, C | 157.2, C |
| 9 | 141.6, C | 141.6, C | 141.6, C |
| 10 | 38.6, C | 38.6, C | 38.6, C |
| 11 | 200.4, C | 200.3, C | 200.2, C |
| 12 | 51.8, CH2 | 51.7, CH2 | 51.6, CH2 |
| 13 | 44.3, C | 44.3, C | 44.4, C |
| 14 | 51.1, C | 51.1, C | 51.1, C |
| 15 | 29.7, CH2 | 29.7, CH2 | 29.7, CH2 |
| 16 | 27.8, CH2 | 27.8, CH2 | 27.6, CH2 |
| 17 | 50.8, CH | 50.8, CH | 50.4, CH |
| 18 | 18.3, CH3 | 18.5, CH3 | 18.5, CH3 |
| 19 | 18.1, CH3 | 18.4, CH3 | 18.1, CH3 |
| 20 | 36.0, CH | 36.1, CH | 36.3, CH |
| 21 | 18.6, CH3 | 18.8, CH3 | 18.9, CH3 |
| 22 | 35.3, CH2 | 30.9, CH2 | 38.0, CH2 |
| 23 | 25.3, CH2 | 32.1, CH2 | 125.1, CH |
| 24 | 124.8, CH | 76.1, C | 139.9, CH |
| 25 | 131.4, C | 147.9, C | 70.9, C |
| 26 | 25.8, CH3 | 111.3, CH2 | 30.1, CH3 |
| 27 | 17.8, CH3 | 17.7, CH3 | 30.1, CH3 |
| 28 | 28.3, CH3 | 28.3, CH3 | 28.3, CH3 |
| 29 | 16.2, CH3 | 16.3, CH3 | 16.2, CH3 |
| 30 | 26.0, CH3 | 26.1, CH3 | 26.0, CH3 |