| Crystal data |
| Chemical formula |
[Ru(C12H14NO2)2(C12H8N2)]PF6
|
|
M
r
|
834.73 |
| Crystal system, space group |
Tetragonal, P41212 |
| Temperature (K) |
173 |
|
a, c (Å) |
15.3094 (13), 15.315 (2) |
|
V (Å3) |
3589.5 (8) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.56 |
| Crystal size (mm) |
0.46 × 0.43 × 0.42 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.638, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
53896, 4516, 3564 |
|
R
int
|
0.067 |
| (sin θ/λ)max (Å−1) |
0.669 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.038, 0.107, 1.04 |
| No. of reflections |
4516 |
| No. of parameters |
245 |
| No. of restraints |
26 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.38, −0.41 |
| Absolute structure |
Flack x determined using 1296 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
−0.003 (14) |
