| Crystal data |
| Chemical formula |
[In2(C18H22NO2)2Cl4(H2O)2] |
|
M
r
|
976.20 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
163 |
|
a, b, c (Å) |
10.297 (4), 10.940 (4), 11.711 (5) |
| α, β, γ (°) |
63.57 (3), 72.47 (3), 62.92 (3) |
|
V (Å3) |
1043.8 (8) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.40 |
| Crystal size (mm) |
0.19 × 0.10 × 0.07 |
| |
| Data collection |
| Diffractometer |
Stoe Stadivari |
| Absorption correction |
Multi-scan (X-RED32; Stoe & Cie, 2002 ▸) |
|
Tmin, Tmax
|
0.766, 0.907 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
62899, 62899, 42801 |
|
R
int
|
0.039 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.039, 0.061, 0.88 |
| No. of reflections |
62899 |
| No. of parameters |
234 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.94, −0.74 |
