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. Author manuscript; available in PMC: 2024 Oct 7.
Published in final edited form as: J Biomol NMR. 2022 Dec 19;77(1-2):1–14. doi: 10.1007/s10858-022-00407-y

Figure 7.

Figure 7.

(A) [1H-1H] WADE-NOESY of UBIK48C with WADE pulses of 3.33 kHz to improve peak detections near the water signal. The highlighted regions emphasize resonances with a significantly higher intensity than those in the ES-NOESY. The experiment was performed on a Bruker 850 MHz spectrometer at 303 K. 128 number of complex points were acquired in indirect dimension and 4 scans per FID with a relaxation delay of 2 sec. (B) 1D slices from near water and far off resonance regions of the spectrum.