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(A) Reaction scheme of the chemical approach to amorphous NixPy via phosphorus insertion. (B) TEM image of Ni nanoparticles synthesized at 215 °C for 60 min via reduction of Ni(acac)2 in OLAM without the presence of TOP. (C–F) TEM images of the products from the reactions under the same conditions at 215 °C for 60 min but varying the molar ratio of TOP/Ni(acac)2: (C) 0.5; (D) 2.5; (E) 5.5; and (F) 11.0.
