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. 2024 Sep 27;63(40):18981–18991. doi: 10.1021/acs.inorgchem.4c03334

Figure 7.

Figure 7

(A) UV–vis spectra of the aliquots taken from the reaction for the synthesis of the amorphous NixPy with 1 mL of TOP used; (B) calculated UV–vis spectrum (λmax = 313 nm) of a tetrahedral Ni(0)-TOP4 complex shown in the inset; and (C) schematic illustration of the reaction mechanism for the TOP-mediated synthesis.