Reuses of MgCl2 (5 mol%) for the intermolecular ketone-ene reaction between α-methyl styrene 1 and methyl pyruvate 2 (1 equivalent) without any solvent at room temperature for 18 h. GC yields.
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|---|---|---|---|---|---|---|---|---|---|---|
| Use | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 |
| Yield (%) | 92 | 86 | 94 | 84 | 84 | 86 | 80 | 82 | 94 | 84 |