TABLE 2.
The determined levels of aromatic volatile compounds present in GT infusions obtained during different brewing amounts and times (%).
| Aroma components | Time (min) | ||||||||
|---|---|---|---|---|---|---|---|---|---|
| 5 | 10 | 15 | |||||||
| GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | |
| n‐Nonanal | (1.81 ± 0.03)ij | – | (2.24 ± 0.01)de | – | – | (2.67 ± 0.03)b | – | (2.06 ± 0.03)fg | – |
| 2‐Decenal | (6.93 ± 0.04)cf | (5.50 ± 0.04)fj | (5.21 ± 0.01)gk | (5.10 ± 0.01)hk | (7.97 ± 0.01)bd | (8.42 ± 0.03)bd | (7.27 ± 0.02)be | (6.81 ± 0.02)dg | (3.65 ± 0.01)kl |
| Isobornyl acetate | (2.37 ± 0.01)b | (2.82 ± 0.02)a | – | (1.64 ± 0.03)c | – | – | – | – | – |
| Unknown 1 | (6.78 ± 0.01)x | (9.60 ± 0.03)n | (6.43 ± 0.02)z | (7.55 ± 0.04)u | (12.65 ± 0.01)d | (5.88 ± 0.04)bl | (11.55 ± 0.07)f | (6.25 ± 0.01)al | (7.02 ± 0.03)w |
| α‐Ionone | (2.72 ± 0.04)no | (3.46 ± 0.01)jk | (5.13 ± 0.01)e | (3.65 ± 0.02)ij | (5.82 ± 0.01)d | (9.17 ± 0.01)b | (11.97 ± 0.01)a | (5.72 ± 0.02)d | (5.79 ± 0.04)d |
| β‐Ionone | (7.75 ± 0.04)p | (9.45 ± 0.04)l | (12.94 ± 0.00)b | (7.39 ± 0.01)rs | (10.97 ± 0.02)g | (17.73 ± 0.04)a | – | (11.70 ± 0.08)e | (9.41 ± 0.01)lm |
| Methoxy‐1‐methylethyl pyrazine | (7.51 ± 0.01)u | (9.20 ± 0.14)q | (10.29 ± 0.03)n | (7.20 ± 0.03)q | (12.55 ± 0.02)g | (15.83 ± 0.02)a | – | (12.52 ± 0.02)g | (8.51 ± 0.02)r |
| Diethyl phthalate | (24.32 ± 0.03)a | (18.15 ± 0.21)j | (22.61 ± 0.03)e | (22.88 ± 0.03)d | (22.25 ± 0.03)f | (23.44 ± 0.03)c | (19.56 ± 0.03)h | (23.95 ± 0.01)b | (15.30 ± 0.01)o |
| Nonadecane | (2.87 ± 0.06)g | – | (2.78 ± 0.01)h | – | – | – | – | – | – |
| Lauric acid | (2.27 ± 0.01)y | (3.98 ± 0.01)m | (4.88 ± 0.05)k | (4.70 ± 0.03)l | (6.04 ± 0.02)f | (6.51 ± 0.01)d | (3.33 ± 0.02)q | (5.44 ± 0.01)h | (3.30 ± 0.02)qr |
| Ethyl salicylate | (2.54 ± 0.06)f | – | – | – | – | – | – | (3.47 ± 0.01)c | – |
| Isopropyl myristate | (7.07 ± 0.04)b | (3.05 ± 0.04)c | (2.14 ± 0.03)e | (4.66 ± 0.04)c | – | – | – | – | – |
| Caffeine | (4.10 ± 0.01)s | (2.22 ± 0.01)w | (4.41 ± 0.03)qr | (5.68 ± 0.01)l | – | – | (5.92 ± 0.04)k | (5.33 ± 0.04)m | (5.94 ± 0.02)k |
| Phytone | (6.78 ± 0.04)t | (5.91 ± 0.01)u | (7.41 ± 0.01)rs | (7.22 ± 0.03)s | (6.89 ± 0.01)t | (7.95p ± .01)p | (8.66 ± 0.01)n | (7.58 ± 0.03)qr | (7.69 ± 0.42)q |
| Theaspirane | (4.90 ± 0.02)e | (4.35 ± 0.02)f | – | (2.26 ± 0.01)k | – | – | (3.90 ± 0.01)g | (6.34 ± 0.02)b | (3.12 ± 0.01)h |
| Palmitic acid | (5.96 ± 0.04)a | – | – | – | – | – | – | – | – |
| Unknown 2 | (3.27 ± 0.02)a | – | – | – | – | – | – | – | – |
| Decanal | (1.82 ± 0.02)c | – | – | – | – | – | – | – | (1.24 ± 0.03)d |
| Unknown 3 | – | (2.13 ± 0.02)d | – | – | (2.55 ± 0.01)a | – | – | – | – |
| Heptadecane | – | (1.62 ± 0.04)e | (1.85 ± 0.01)d | – | – | – | – | – | – |
| Unknown 4 | – | (4.30 ± 0.03)c | ‐ | – | (3.40 ± 0.03)e | – | (8.33 ± 0.01)a | ‐ | (3.25 ± 0.01)f |
| Hexadecane | (2.93 ± 0.04)e | – | ‐ | – | – | – | – | (3.05 ± 0.03)d | – |
| Methyl palmitate | – | (1.67 ± 0.01)e | (1.96 ± 0.04)d | (1.63 ± 0.03)e | (2.72 ± 0.03)a | – | – | – | – |
| Butyl laurate | – | (3.74 ± 0.03)a | – | – | – | – | – | – | – |
| ω‐Pentadecalactone | – | (1.63 ± 0.00)b | – | (1.97 ± 0.01)a | – | – | (2.01 ± 0.03)a | – | (1.76 ± 0.03)b |
| Nonanoic acid | – | – | (2.22 ± 0.01)t | – | – | – | – | – | (7.83 ± 0.01)i |
| Unknown 5 | – | (5.01 ± 0.02)j | – | (6.42 ± 0.02)d | – | – | – | – | – |
| Lauryl alcohol | – | – | – | (1.82 ± 0.01)a | – | – | – | – | – |
| Eicosane | – | – | – | (3.87 ± 0.01)e | (4.27 ± 0.03)c | (2.43 ± 0.02)g | – | – | – |
| Unknown 6 | – | – | – | (2.23 ± 0.03)b | – | – | – | – | (1.35 ± 0.03)c |
| Isoamyl benzoate | – | – | – | (1.96 ± 0.01)g | (1.99 ± 0.03)g | – | – | – | (2.64 ± 0.02)de |
| 3‐Methyl‐2‐(n‐pentanyl)‐2‐cyclopenten‐1‐one | – | – | – | – | – | – | (11.63 ± 0.04)a | – | – |
| 5‐Hydroxy‐2,4‐decadienoic acid δ‐lactone | – | – | – | – | – | – | – | – | (1.14 ± 0.03)a |
| Unknown 7 | – | – | – | – | – | – | – | – | (3.67 ± 0.03)a |
| 6‐Methyl‐5‐hepten‐2‐one | – | – | – | – | – | – | – | – | (1.47 ± 0.01)a |
| Octadecane | – | – | – | – | – | – | – | – | (1.57 ± 0.02)j |
| Butylated hydroxytoluene | – | – | – | – | – | – | – | – | (10.21 ± 0.04)b |
| Tetrahydrofurfuryl butyrate | – | – | – | – | – | – | – | (10.47 ± 0.00)a | – |
| Aroma components | Time (min) | ||||||||
|---|---|---|---|---|---|---|---|---|---|
| 20 | 25 | 30 | |||||||
| GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | |
| n‐Nonanal | – | (0.77 ± 0.02)l | – | – | (0.90 ± 0.02)l | (2.01 ± 0.00)gh | – | (2.00 ± 0.01)g | – |
| 2‐Decenal | (5.46 ± 0.01)hk | (4.17 ± 0.01)jk | (4.43 ± 0.02)ik | (4.95 ± 0.02)hk | (3.75 ± 0.01)kl | (5.01 ± 0.04)hk | (4.71 ± 0.02)hk | (6.00 ± 0.02)ei | (6.88 ± 0.02)df |
| Unknown 1 | (9.95 ± 0.01)l | (6.49 ± 0.02)z | (7.37 ± 0.01)v | (10.33 ± 0.04)k | (7.65 ± 0.01)t | (8.23 ± 0.02)r | (10.98 ± 0.03)h | (11.82 ± 0.01)e | (5.03 ± 0.02)cl |
| α‐Ionone | (3.37 ± 0.04)jl | (3.54 ± 0.03)j | (3.95 ± 0.03)hi | (2.51 ± 0.01)op | (3.92 ± 0.03)hi | (4.58 ± 0.01)f | (3.22 ± 0.02)km | (2.22 ± 0.03)pq | (3.92 ± 0.01)hi |
| β‐Ionone | (7.15 ± 0.02)t | (6.24 ± 0.02)w | (8.94 ± 0.01)n | (6.44 ± 0.04)v | (7.20 ± 0.01)st | (9.83 ± 0.01)k | (7.66 ± 0.01)pq | (6.82 ± 0.03)u | (9.83 ± 0.01)k |
| Methoxy‐1‐methylethyl pyrazine | (8.14 ± 0.01)s | (6.15 ± 0.01)y | (10.08 ± 0.03)o | (6.63 ± 0.01)x | (7.01 ± 0.03)w | (11.45 ± 0.00)k | (9.64 ± 0.03)p | (9.57 ± 0.01)p | (11.73 ± 0.01)j |
| Diethyl phthalate | (17.36 ± 0.04)l | (11.76 ± 0.24)w | (17.37 ± 0.04)l | (12.90 ± 0.02)t | (11.84 ± 0.02)w | (14.27 ± 0.01)q | (21.67 ± 0.39)g | (14.64 ± 0.02)p | (18.00 ± 0.03)jk |
| Nonadecane | (4.84 ± 0.02)c | – | – | – | – | (4.43 ± 0.01)f | – | – | (4.42 ± 0.03)e |
| Lauric acid | – | (5.27 ± 0.01)i | (4.71 ± 0.01)l | (4.83 ± 0.11)k | (3.68 ± 0.04)n | (3.58 ± 0.01)o | (2.55 ± 0.03)w | (4.98 ± 0.02)j | (3.58 ± 0.02)o |
| Ethyl salicylate | – | (4.54 ± 0.04)b | (2.66 ± 0.01)e | (3.08 ± 0.01)d | (2.33 ± 0.03)g | – | – | – | – |
| Isopropyl myristate | – | – | – | – | – | – | – | – | (8.15 ± 0.01)a |
| Caffeine | (8.04 ± 0.03)c | (5.14 ± 0.02)n | (3.96 ± 0.03)t | (4.81 ± 0.01)p | (4.14 ± 0.04)s | (6.55 ± 0.01)g | (7.20 ± 0.01)e | (5.64 ± 0.01)l | (6.42 ± 0.03)h |
| Phytone | (8.27 ± 0.04)o | (5.67 ± 0.02)v | (8.12 ± 0.01)op | (8.12 ± 0.02)op | (8.02 ± 0.01)p | (9.55 ± 0.02)ij | (9.86 ± 0.01 g)h | (9.13 ± 0.01)lm | (8.25 ± 0.04)o |
| Theaspirane | (3.64 ± 0.03)a | (9.41 ± 0.01)a | (5.43 ± 0.03)d | (5.96 ± 0.02)c | (3.52 ± 0.01)i | (2.19 ± 0.01)l | – | – | – |
| Decanal | – | – | (1.12 ± 0.01)e | – | – | – | – | – | (1.75 ± 0.03)c |
| Unknown 3 | (2.17 ± 0.04)d | (1.34 ± 0.01)i | – | – | (1.46 ± 0.02)h | ‐ | (2.03 ± 0.01)e | (1.73 ± 0.03)f | – |
| Heptadecane | – | – | – | – | ‐ | (1.42 ± 0.03)f | (2.04 ± 0.04)c | ‐ | – |
| Unknown 4 | (2.61 ± 0.04)h | – | – | – | (3.65 ± 0.04)d | – | – | (5.15 ± 0.02)b | – |
| Hexadecane | – | (2.35 ± 0.03)g | – | – | – | – | – | – | – |
| Methyl palmitate | – | (2.63 ± 0.03)b | (2.17 ± 0.01)c | (1.51 ± 0.01)f | – | – | – | – | – |
| Butyl laurate | – | – | – | – | – | – | – | – | – |
| ω‐Pentadecalactone | – | – | – | – | – | – | – | – | – |
| Nonanoic acid | (9.83 ± 0.03)c | (4.31 ± 0.04)p | (6.52 ± 0.03)j | (8.63 ± 0.01)f | (8.53 ± 0.01)g | (11.95 ± 0.03)p | (4.50 ± 0.02)o | (6.54 ± 0.04)j | (4.25 ± 0.03)gj |
| Unknown 5 | (7.96 ± 0.01)a | – | (6.28 ± 0.03)e | – | ‐ | (5.53 ± 0.03)f | (7.21 ± 0.04)b | – | – |
| Lauryl alcohol | – | – | – | – | (1.24 ± 0.04)b | – | ‐ | – | – |
| Eicosane | – | – | (4.03 ± 0.01)d | – | (2.94 ± 0.03)f | – | (1.36 ± 0.02)h | – | – |
| Unknown 6 | – | (1.05 ± 0.01)d | – | – | – | – | – | – | – |
| Isoamyl benzoate | – | (4.54 ± 0.04)a | – | (2.24 ± 0.01)f | (2.59 ± 0.02)e | – | ‐ | (2.67 ± 0.02)d | – |
| Octadecane | – | – | – | (3.30 ± 0.03)h | – | – | (4.76 ± 0.01)e | (4.22 ± 0.02)g | (1.35 ± 0.01)k |
| Butylated hydroxytoluene | – | (7.71 ± 0.02)c | – | (5.31 ± 0.02)f | (5.73 ± 0.02)e | – | – | – | (4.94 ± 0.02)g |
| Geranyl acetone | (1.65 ± 0.03)a | – | – | – | – | – | – | – | – |
| Linalool | – | – | – | – | (1.01 ± 0.01)a | ‐ | – | – | – |
| Tetrahydrofurfuryl butyrate | – | (1.90 ± 0.02)d | – | (4.92 ± 0.02)b | (2.76 ± 0.01)c | – | – | – | – |
| Pentacosane | – | (1.82 ± 0.03)a | – | – | – | – | – | – | – |
| Pentadecane | – | – | (1.41 ± 0.01)f | – | – | – | (2.35 ± 0.04)b | (1.67 ± 0.02)e | – |
| Isopulegyl acetate | – | – | – | (1.78 ± 0.02)a | (1.61 ± 0.03)b | – | – | – | – |
| Tetradecane | – | – | – | – | (0.97 ± 0.01)d | – | – | – | – |
| Docosane | – | – | – | – | (1.47 ± 0.001)a | – | – | – | – |
| Decyl propionate | – | – | – | – | – | – | – | (1.67 ± 0.02)a | – |
| Aroma components | Time (min) | ||||||||
|---|---|---|---|---|---|---|---|---|---|
| 35 | 40 | 45 | |||||||
| GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | |
| n‐Nonanal | (1.67 ± 0.03)j | – | – | (2.35 ± 0.07)ce | (1.80 ± 0.14)ij | – | – | (2.37 ± 0.01)cd | (2.79 ± 0.01)ab |
| 2‐Decenal | (6.10 ± 0.02)eh | (7.04 ± 0.01)cf | (7.34 ± 0.03)be | (7.53 ± 0.02)be | (7.75 ± 0.04)bd | (5.16 ± 0.03)hk | (2.33 ± 0.02)l | (11.75 ± 0.01)a | (4.82 ± 0.51)hk |
| Unknown 1 | (9.72 ± 0.03)m | ‐ | (8.33 ± 0.02)q | (5.85 ± 0.01)bl | (8.25 ± 0.02)r | (10.82 ± 0.02)i | (11.23 ± 0.04)g | (6.68 ± 0.03)y | (9.06 ± 0.03)o |
| α‐Ionone | (3.91 ± 0.01)hi | (3.66 ± 0.01)ij | (5.06 ± 0.53)e | (3.65 ± 0.02)ij | (4.43 ± 0.01)fg | (5.16 ± 0.00)e | (2.07 ± 0.01)qr | (5.32 ± 0.04)e | (3.11 ± 0.02)lm |
| β‐Ionone | (7.44 ± 0.01)r | (10.70 ± 0.08)h | (12.34 ± 0.04)c | (7.47 ± 0.01)qr | (10.92 ± 0.03)g | (9.38 ± 0.01)lm | (4.90 ± 0.01)x | (12.13 ± 0.03)d | (10.34 ± 0.00)i |
| Methoxy‐1‐methylethyl pyrazine | (7.67 ± 0.02)t | (11.23 ± 0.01)l | (14.01 ± 0.03)d | (9.62 ± 0.01)p | (10.46 ± 0.02)m | (11.95 ± 0.01)l | (7.14 ± 0.01)v | – | (12.44 ± 0.01)gh |
| Diethyl phthalate | (19.17 ± 0.01)i | (12.23 ± 0.01v | (14.54 ± 0.03)p | (16.62 ± 0.01)m | (12.24 ± 0.02)v | (11.15 ± 0.01)x | (13.34 ± 0.03)s | (17.82 ± 0.01)k | (13.87 ± 0.02)r |
| Nonadecane | – | – | – | – | (4.74 ± 0.02)d | – | – | – | – |
| Lauric acid | (4.97 ± 0.02)j | (3.54 ± 0.04)o | (2.67 ± 0.04)u | (5.75 ± 0.03)g | (3.52 ± 0.01)o | (5.35 ± 0.02)i | (3.24 ± 0.01)rs | (6.76 ± 0.01)e | (3.17 ± 0.01)s |
| Isopropyl myristate | (1.42 ± 0.01)f | – | – | – | – | – | – | – | – |
| Caffeine | (3.76 ± 0.02)u | 10.54 ± 0.03)a | (6.33 ± 0.01)l | (4.45 ± 0.01)q | (8.35 ± 0.00)b | (6.06 ± 0.04)j | (4.91 ± 0.04)o | – | – |
| Phytone | (9.74 ± 0.01)hi | (12.62 ± .03)ab | (12.78 ± 0.03)a | (12.53 ± 0.04)b | (10.54 ± 0.04)b | (9.37 ± 0.01)jk | (8.73 ± 0.01)n | (9.01 ± 0.02)m | (10.16 ± 0.01)ef |
| Decanal | – | (2.14 ± 0.01)a | – | – | – | (2.03 ± 0.02)b | ‐ | – | – |
| Unknown 3 | – | – | – | – | – | (1.61 ± 0.01)g | (2.33 ± 0.03)c | – | – |
| Heptadecane | (3.86 ± 0.01)a | – | (2.16 ± 0.03)b | – | – | – | ‐ | – | – |
| Unknown 4 | – | – | – | – | (2.27 ± 0.04)i | – | (4.37 ± 0.01)c | – | – |
| Hexadecane | – | – | – | – | – | – | (4.76 ± 0.01)b | – | – |
| Nonanoic acid | (2.45 ± 0.03)s | (6.22 ± 0.04)k | (6.53 ± 0.02)j | (9.30 ± 0.03)d | (9.85 ± 0.02)c | (11.55 ± 0.01)b | (8.36 ± 0.01)h | – | (5.43 ± 0.04)m |
| Unknown 5 | (5.32 ± 0.02)h | (6.65 ± 0.04)c | (3.86 ± 0.04)l | – | (5.14 ± 0.01)i | (5.35 ± 0.02)h | – | (2.99 ± 0.03)n | – |
| Lauryl alcohol | – | – | – | – | – | – | – | – | – |
| Eicosane | – | – | (4.73 ± 0.03)b | (7.83 ± 0.03)a | – | – | – | – | – |
| Isoamyl benzoate | – | – | – | – | – | – | (3.79 ± 0.03)b | – | – |
| Octadecane | – | – | – | – | – | (5.02 ± 0.01)d | ‐ | (1.72 ± 0.03)i | (6.52 ± 0.02)b |
| Butylated hydroxytoluene | – | – | – | (6.88 ± 0.03)d | – | – | (4.84 ± 0.02)h | – | (3.23 ± 0.03)j |
| Pentadecane | – | – | – | – | – | (2.14 ± 0.01)d | (1.75 ± 0.02)e | – | (2.50 ± 0.04)a |
| Isopulegyl acetate | – | – | – | – | – | – | (1.61 ± 0.01)b | – | – |
| Tetradecane | – | – | – | – | – | – | – | – | (2.17 ± 0.01)b |
| Octyl octanoate | – | (3.00 ± 0.01)a | – | – | – | – | – | – | – |
| α‐Cubebene | (2.90 ± 0.01)a | – | – | – | – | – | – | – | – |
| Pulegone | – | – | – | – | – | – | – | (17.14 ± 0.02)a | – |
| Neodene | – | – | – | – | – | – | – | – | (1.75 ± 0.01)a |
| cis‐8‐Undecenal | – | – | – | (2.35 ± 0.04)b | (1.71 ± 0.03)d | (1.16 ± 0.01)f | – | (3.23 ± 0.00)a | – |
| Aroma components | Time (min) | ||||||||
|---|---|---|---|---|---|---|---|---|---|
| 50 | 55 | 60 | |||||||
| GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | GT1 | GT2 | GT3 | |
| n‐Nonanal | (1.81 ± 0.01)ij | (2.20 ± 0.14)ef | (2.87 ± 0.03)a | – | – | (2.45 ± 0.01)c | (1.45 ± 0.01)k | (1.83 ± 0.03)hi | (2.80 ± 0.04)ab |
| 2‐Decenal | (8.77 ± 0.01)b | (7.26 ± 0.01)be | (8.16 ± 0.01)bd | – | (7.34 ± 0.00)be | (8.54 ± 0.01)bc | (4.45 ± 0.01)ij | (7.19 ± 0.03)be | (6.92 ± 0.03)df |
| Isobornyl acetate | – | – | – | – | – | – | – | – | – |
| Unknown 1 | (13.95 ± 0.02)c | (10.46 ± 0.01)j | (10.97 ± 0.00)h | (7.77 ± 0.01)s | (17.45 ± 0.04)a | (14.67 ± 0.01)b | ‐ | ‐ | (8.62 ± 0.01)p |
| α‐Ionone | ‐ | (5.21 ± 0.01)e | (3.09 ± 0.01)lm | (6.36 ± 0.01)c | (1.88 ± 0.04)r | (3.65 ± 0.01)ij | (3.09 ± 0.03)lm | (4.13 ± 0.01)gh | (2.92 ± 0.03)mn |
| β‐Ionone | (7.97 ± 0.03)o | (10.67 ± 0.01)h | (10.10 ± 0.02)j | (12.42 ± 0.01)c | (7.84 ± 0.04o)p | (10.12 ± 0.01)j | (7.21 ± 0.02)st | (9.23 ± 0.01)m | (9.67 ± 0.029)k |
| Methoxy‐1‐methylethyl pyrazine | (12.40 ± 0.14)h | (13.04 ± 0.03)f | (14.55 ± 0.03)c | (13.02 ± 0.01)f | (13.43 ± 0.02)e | (15.34 ± 0.00)b | – | (9.64 ± 0.03)p | (11.73 ± 0.02)j |
| Diethyl phthalate | (22.60 ± 0.01)e | (13.79 ± 0.01)r | (12.56 ± 0.04)u | (17.45 ± 0.01)l | (15.81 ± 0.00)n | (9.46 ± 0.02)y | (15.62 ± 0.03)n | – | (13.48 ± 0.01)s |
| Nonadecane | – | (5.84 ± 0.03)b | (6.26 ± 0.02)a | – | – | – | – | (4.41 ± 0.01)e | (2.22 ± 0.02)j |
| Lauric acid | (2.32 ± 0.03)yx | (7.13 ± 0.03)b | (6.27 ± 0.01)e | (3.41 ± 0.01)p | (2.36 ± 0.01)x | (8.19 ± 0.00)a | (2.46 ± 0.03)w | (3.27 ± 0.03)qr | (3.04 ± 0.02)t |
| Ethyl salicylate | – | – | – | – | (7.42 ± 0.01)a | – | – | – | – |
| Caffeine | (3.20 ± 0.02)v | – | – | (6.79 ± 0.02)f | (7.74 ± 0.04)d | (4.37 ± 0.01)r | – | – | – |
| Phytone | (10.17 ± 0.02)ef | (12.56 ± 0.02)b | (10.12 ± 0.03)ef | (10.76 ± 0.03)c | (10.12 ± 0.01)fg | (10.25 ± 0.02)e | (8.56 ± 0.03)n | (8.64 ± 0.01)n | (9.24 ± 0.01)kl |
| Unknown 3 | – | – | (2.47 ± 0.01)b | – | (2.57 ± 0.01)a | (1.63 ± 0.01)g | – | – | – |
| Heptadecane | – | – | – | – | – | – | – | – | – |
| Unknown 4 | (2.77 ± 0.02)g | – | – | – | – | (2.30 ± 0.01)i | (1.76 ± 0.01)j | – | (2.81 ± 0.03)g |
| Hexadecane | (6.56 ± 0.03)a | – | – | – | – | (2.46 ± 0.03)f | (4.54 ± 0.04)c | (1.42 ± 0.01)i | – |
| Nonanoic acid | (5.53 ± 0.01)l | – | (3.93 ± 0.02)q | (2.73 ± 0.02)r | – | (1.37 ± 0.01)u | (4.43 ± 0.03)o | (9.22 ± 0.02)e | (5.12 ± 0.02)n |
| Unknown 5 | (3.21 ± 0.01)m | – | – | – | (1.85 ± 0.03)p | (2.66 ± 0.03)o | – | (4.75 ± 0.01)k | – |
| Unknown 6 | – | – | – | – | – | (2.85 ± 0.03)a | – | – | – |
| Octadecane | – | (3.55 ± 0.04)g | – | – | (7.83 ± 0.03)a | – | – | – | (6.24 ± 0.04)c |
| Butylated hydroxytoluene | – | (3.58 ± 0.04)i | (2.38 ± 0.01)l | (13.30 ± 0.01)a | ‐ | – | (6.90 ± 0.03)d | – | (3.03 ± 0.01)k |
| Pentadecane | – | – | (2.24 ± 0.03)c | ‐ | ‐ | – | (2.29 ± 0.02)bc | – | (2.43 ± 0.03)a |
| Tetradecane | – | – | (2.14 ± 0.02)b | ‐ | ‐ | (1.52 ± 0.02)c | – | (0.94 ± 0.01)d | (2.12 ± 0.03)b |
| Decyl propionate | – | – | (0.29 ± 0.00)b | ‐ | ‐ | ‐ | – | – | – |
| 3,7‐Dimethyl‐1‐octanol | – | – | – | – | (1.70 ± 0.01)a | ‐ | – | – | – |
| Davanone B | – | – | – | – | – | – | (9.12 ± 0.01)a | – | – |
| cis‐8‐Undecenal | (2.07 ± 0.02)c | – | (2.00 ± 0.03)c | – | – | (1.54 ± 0.03)e | ‐ | – | – |
| 2‐Undecenal | – | – | – | – | – | – | – | (1.71 ± 0.04)a | – |
| Methyl anthranilate | – | – | – | – | – | – | – | (11.27 ± 0.02)a | – |
| Di‐isobutyl phthalate | – | – | – | – | – | – | (4.60 ± 0.04)a | (2.02 ± 0.02)b | – |
| 2‐Octenal | – | – | – | – | – | – | – | (1.94 ± 0.03)a | – |
Note: Results are expressed as mean value±standard deviation (n = 2). Different letters in superscript within rows show significant differences (p ≤ .01); GT1, GT2, and GT3 indicate 5, 7.5, and 10 g samples, respectively; − indicates not detected aroma component.