Table 2. Chemical Shifts (ppm) of 1-R and 3-R and 1JP–Se Coupling Constants (Hertz) of 3-R Determined by 31P{1H} NMR Spectroscopy in Toluene-d8.
| R | δ/ppm (1-R) | δ/ppm (3-R) | 1JP–Se/Hz (3-R) |
|---|---|---|---|
| NMe2 | 107.8 | 108.8 | 794 |
| OMe | 111.7 | 112.0 | 801 |
| Me | 113.4 | 113.3 | 804 |
| H | 115.1 | 114.1 | 806 |
| F | 115.2 | 114.4 | 806 |
| CF3 | 119.7 | 116.4 | 810 |