Skip to main content
. 2024 Nov 1;14(47):34925–34937. doi: 10.1039/d4ra05774k

Reaction rate and photonic efficiency for the bromination of 6-chloro-3-methyluracil at Δt = 0–720 s concerning different reaction modules and reaction scales.

Entry Reactor module Reaction scale (g) Reaction volume (mL) Applied photon flux (μmol s−1) % yield Δt (s) Rate (μmol s−1) Photonic efficiency (ξext)
1 1XA 0.96 10 46 94 0–720 6.2 0.13
2 2XA 4.8 50 102 93 0–720 31 0.30
3 4XA 9.6 100 185 94 0–720 62 0.34