Table 5.
Residues (mg kg−1) of fipronil and its metabolites in chilli fruits at the lower dose (40 g a.i. ha−1).
| Days | Control |
Fipronil |
Desulfinyl (MB046513) |
Sulfide (MB045950) |
Sulfone (MB046136) |
Total |
|---|---|---|---|---|---|---|
| Meana± SD | Meanb± SD | Meanb± SD | Meanb± SD | |||
| 0 | ND | 0.574 ± 0.002 (0.0)a | 0.123 ± 0.002 (0.0) | 0.031 ± 0.002 (0.0) | 0.180 ± 0.004 (0.0) | 0.908 (0.0) |
| 1 | ND | 0.380 ± 0.002 (33.8) | 0.101 ± 0.002 (17.9) | 0.019 ± 0.003 (38.7) | 0.137 ± 0.003 (23.9) | 0.637 (29.8) |
| 3 | ND | 0.238 ± 0.016 (58.5) | 0.074 ± 0.003 (39.8) | 0.006 ± 0.001 (80.6) | 0.066 ± 0.003 (63.3) | 0.384 (57.7) |
| 5 | ND | 0.182 ± 0.003 (68.3) | 0.044 ± 0.002 (64.2) | 0.002 ± 0.001 (93.5) | 0.020 ± 0.001 (88.9) | 0.248 (72.7) |
| 7 | ND | 0.064 ± 0.003 (88.9) | 0.015 ± 0.003 (87.8) | BDL | 0.006 ± 0.001 (96.7) | 0.085 (90.6) |
| 10 | ND | 0.023 ± 0.004 (96.1) | BDL | – | BDL | 0.023 (97.5) |
| 15 | ND | BDL | – | – | – | BDL |
| Correlation Coefficient R2 = 0.974 | Correlation Coefficient R2 = 0.937 | Correlation Coefficient R2 = 0.998 | Correlation Coefficient R2 = 0.985 Regression Equation y = -0.212x + 1.348 RL50 = 2.2 Waiting Period (Days) = 5 |
|||
| Regression eq. Log Y = −0.136x + 1.780 | Regression Equation y = −0.123x + 1.156 | Regression Equation y = -0.232x + 0.498 | ||||
| RL50 = 3.4 | RL50 = 3.8 | RL50 = 1.2 | ||||
| Waiting Period (Days) = 7 | Waiting Period (Days) = 5 | Waiting Period (Days) = 3 | ||||
% reduction of four replications.
Mean of four replications BDL = Below Determination Level ND=Not Detected.