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. 2024 Nov 15;14(49):36527–36537. doi: 10.1039/d4ra03674c

1H NMR, and 13C NMR data of compound (1 and 2) in CDCl3.

Compound 1 Compound 2
Position δ H δ C Position δ H δ C
1 3.43, m 71.2
2 2.92, 2.99, dd 47.1 3 1.48, 1.23, m 30.6
3 197.5 4 1.27,0.99, m 36.3
4 107.8 5 2.16,1.86, dd 38.3
5 160.1 6 138.4
6 110.2 7 5.23, d 116.4
7 141.2 8 5.23, d 116.7
8 6.90, s 99.2 9 139.6
9 153.4 10 1.88, m 52.1
11 6.73, s 104.1 11 1.49, 1.40, m 21.1
12 165.4 12 1.88, m 25.6
13 103.1 13 1.08, m 54.5
14 150.6 14 1.96, m 38.8
16-CH3 1.42, s 27.5 15 5.11, m 131.4
18-OCH3 3.80, s 55.2 16 5.1, m 129.5
20-OCH3 4.00, s 61.63 17 1.88, m 38.5
21-OH 14.21 18 0.85, s 18.2
22-OH 5.60 19 1.49, m 31.23
23 100.5 20 0.98, m 19.5
24 2.92,2.99, dd 47.1 21 0.98 19.1
25 197.5 22 0.84, s 19.3
26 108.3 23 41.7
27 158.8 24 1.03, m 13.5
28 111.3 25 1.15, m 37.3
29 136.5 26 0.89, m 19.3
30 112.6 27 1.79, m 43.6
31 155.8 28 34.7
33 6.43, s 97.2 29 0.93, s 14.6
34 163.7
35 6.21, s 96.2
36 160.6
38-CH3 1.52, s 27.5
40-OCH3 3.99, s 56.2
42-OCH3 3.81, s 55.9
43-OH 14.56
44-OH 7.12