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. 2024 Oct 31;13(11):1338. doi: 10.3390/antiox13111338

Table 2.

13C NMR (150 MHz) data of compounds 15 (CDCl3).

Carbon 1 2 3 4 5
1 38.6 71.8 71.1 77.2 70.6
2 35.1 30.3 25.1 24.5 29.1
3 217.0 73.6 73.1 72.4 72.2
4 47.7 42.5 43.9 43.9 42.4
5 52.5 40.2 38.7 38.7 39.0
6 24.5 72.9 73.7 73.9 72.5
7 118.2 74.7 74.1 74.0 74.6
8 145.7 44.5 39.7 39.8 45.4
9 48.0 36.6 34.3 34.8 36.4
10 35.2 40.3 45.2 45.2 41.2
11 17.9 34.1 30.5 30.4 30.5
12 31.6 213.8 77.9 71.2 97.8
13 43.6 61.5 52.5 51.7 140.3
14 50.9 154.1 156.1 157.1 146.1
15 34.4 123.8 122.5 122.2 77.9
16 27.6 34.2 35.5 35.8 35.8
17 48.5 42.9 51.2 48.9 49.3
18 23.3 19.4 15.5 15.1 16.5
19 12.8 15.6 16.1 15.5 16.7
20 47.1 124.6 169.1 137.5 _ a
21 101.8 142.4 99.1 171.4 98.7
22 33.6 112.6 120.4 146.5 118.7
23 76.7 141.0 170.9 96.5 170.8
24 86.5
25 71.1
26 25.9
27 25.7
28 24.6 78.1 78.4 78.4 78.1
29 21.7 18.8 20.2 20.2 19.0
30 27.4 25.8 26.7 26.9 20.7
12-OCH3 55.2
1-OAC 170.8
21.2
3-OAC 169.2 170.7
20.9 21.3
12-OAC 170.9
21.5
1’ 165.1 165.4 165.4 166.7
2’ 130.5 117.0 117.2 128.6
3’ 129.6 146.8 144.8 137.5
4’ 128.6 133.8 134.1 14.6
5’ 133.2 128.4 128.5 12.2
6’ 128.6 129.2 129.2
7’ 129.6 131. 130.9
8’ 129.2 129.2
9’ 128.4 128.5

a Signal not clearly observable from 1D and 2D NMR.