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. 2024 Sep 19;23(12):1654–1663. doi: 10.1038/s41563-024-02002-y

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© The Author(s) 2024

Open Access This article is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License, which permits any non-commercial use, sharing, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if you modified the licensed material. You do not have permission under this licence to share adapted material derived from this article or parts of it. The images or other third party material in this article are included in the article’s Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by-nc-nd/4.0/.

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Fig. 6 — a, O1s peak area evolution of PtO₂ and PtO₃–Pt in Fig. 1c as a function of temperature. The insets show the O1s spectra under different stages. b, LEED pattern of the clean Pt(111) surface. c–e, Corresponding LEED patterns at stage I (c), stage II (d) and stage IV (e). f,g, STM images collected at stage II (f) and stage III (g) in a. i–l, Atomic models during the oxidation process. Tunnelling parameters: (f) V_s = 500 mV, I = 0.14 nA; (g) V_s = 1.5 V, I = 0.21 nA; g(i) V_s = 1.5 V, I = 0.21 nA; g(ii) V_s = 1.5 V, I = 0.21 nA; (h) V_s = 2.6 V, I = 0.18 nA.

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