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. 2024 Nov 13;9(47):47065–47076. doi: 10.1021/acsomega.4c07336

Table 2. 13C NMR Spectroscopic Data for Compounds 15 in MeOD.

  1a 2a 3a 4a 5b
position δC δC δC δC δC
1 126.7, C 132.3, C 131.0, C 124.2, C 124.2, C
2 108.8, CH 104.8, CH 104.7, CH 109.1, CH 109.1, CH
3 139.0, C 149.4, C 149.5, C 149.3, C 149.3, C
4 149.2, C 136.6, C 136.7, C 143.3, C 143.2, C
5 139.0, C 149.4, C 149.5, C 146.9, C 147.0, C
6 108.8, CH 104.8, CH 104.7, CH 125.2, C 125.3, C
7 142.3, CH 86.3, CH 86.4, CH 135.4, CH 135.0, CH
8 127.4, C 60.3, CH 60.6, CH 126.8, C 127.1, C
9 168.2, C 172.5, C 172.1, C 170.3, C 170.0, C
1′ 126.7, C 132.3, C 132.4, C 135.3, C 135.2, C
2′ 108.9, CH 104.8, CH 104.9, CH 106.0, CH 106.1, CH
3′ 139.1, C 149.4, C 149.4, C 149.0, C 149.0, C
4′ 149.2, C 136.6, C 136.7, C 135.3, C 135.3, C
5′ 139.1, C 149.4, C 149.4, C 149.0, C 149.5, C
6′ 108.9, CH 104.8, CH 104.9, CH 106.0, CH 106.1, CH
7′ 142.5, CH 86.3, CH 86.4, CH 41.4, CH 41.4, CH
8′ 127.6, C 60.3, CH 60.3, CH 50.2, CH 50.1, CH
9′ 168.2, C 172.5, C 172.5, C 174.3, C 174.2, C
1″ 134.2, C 134.2, C 130.8, C 134.7, C 131.4, C
2″ 128.4, CH 128.5, CH 130.7, CH 128.4, CH 130.7, CH
3″ 116.0, CH 116.1, CH 116.2, CH 116.1, CH 116.2, CH
4″ 158.0, C 158.0, C 156.9, C 158.0, C 156.8, C
5″ 116.0, CH 116.1, CH 116.2, CH 116.1, CH 116.2, CH
6″ 128.4, CH 128.5, CH 130.7, CH 128.4, CH 130.7, CH
7″ 73.0, CH 73.1, CH 35.7, CH2 73.4, CH 35.6, CH2
8″ 48.5, CH2 48.1, CH2 42.6, CH2 48.4, CH2 42.8, CH2
1‴ 134.3, C 134.2, C 134.5, C 134.3, C 134.4, C
2‴ 128.3, CH 128.5, CH 128.5, CH 128.4, CH 130.8, CH
3‴ 116.1, CH 116.1, CH 116.1, CH 116.1, CH 116.2, CH
4‴ 158.0, C 158.0, C 158.0, C 157.9, C 156.9, C
5‴ 116.1, CH 116.1, CH 116.1, CH 116.1, CH 116.2, CH
6‴ 128.3, CH 128.5, CH 128.5, CH 128.4, CH 130.8, CH
7‴ 73.5, CH 73.1, CH 73.2, CH 72.8, CH 72.8, CH
8‴ 48.5, CH2 48.1, CH2 48.1, CH2 48.0, CH2 47.9, CH2
OCH3-3′, 5′ 56.7, CH3 56.8, CH3 56.9, CH3 56.7, CH3 56.7, CH3
OCH3-3 56.7, CH3 56.8, CH3 56.8, CH3 56.8, CH3 56.8, CH3
OCH3-5 56.7, CH3 56.8, CH3 56.8, CH3 60.8, CH3 60.8, CH3
a

Measured at 100 MHz.

b

Measured at 125 MHz.