Table 10.

Main parameters about the XRD acquisitions.

Instrument	Philips X'Pert Pro Diffractometer (Almelo, The Netherlands) working with parafocusing Bragg Brentano geometry
X-ray tube	Long Fine Focus, Co source, 40 kV and 40 mA generator settings
Detector	Real-Time Multiple Strip (RTMS) X'Celerator
Sample holder	Circular, 27 mm diameter and 2 mm thick. Back-loading filling
Accessories	Bragg-BrentanoHD ©, spinner for sample revolution on vertical axis
Slits	Divergence slits 1/4°, antiscatter slits 1°, Soller silits 0.04 rad
Data acquisition	3–85° 2theta, continous scan lasting 1 h (100 s for 0.017° 2theta virtual steps).
Micronization procedure	5 min grinding using ethanol at 1500 rpm/min. Instrument: Retsch XRD-MILL MCCRONE.
Dry grinding procedure	3 min dry grinding at 20 Hz frequency. Instrument: Retsch MM 400
Qualitative phase analysis	HighScore (Plus) software version 4.9, year 2020, by PANalytical B.V., Almelo, The Netherlands [13]
Quantitative phase analysis	Profex-BGMN v.5.2.3 [14]