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. 2024 Jun 6;45(23):2400345. doi: 10.1002/marc.202400345

Table 1.

Molar ratios of the different starting materials for the synthesis of Lin1 to Mel5.0 following the described procedure, with the mass of Mel/Dop/PPG (mMel/Dop/PPG), the amount of substance of Mel/Dop/PPG (nMel/Dop/PPG) and the molar equivalents given as mMel/Dop/PPG.

mMel [mg] nMel [mmol] Mel [eq.] mDop [mg] nDop [mmol] Dop [eq.] mPPG [mg] nPPG [mmol] PPG [eq.] Yield [%]
Lin1 0.00 0.00 0.0 82.2 0.43 3.0 1000 0.43 3.0 93
Mel1.0 18.3 0.14 1.0 82.2 0.43 3.0 1000 0.43 3.0 97
Mel1.5 27.4 0.22 1.5 82.2 0.43 3.0 1000 0.43 3.0 91
Mel2.0 36.6 0.29 2.0 82.2 0.43 3.0 1000 0.43 3.0 94
Mel2.5 45.7 0.36 2.5 82.2 0.43 3.0 1000 0.43 3.0 96
Mel3.0 54.8 0.43 3.0 82.2 0.43 3.0 1000 0.43 3.0 93
Mel3.5 64.0 0.51 3.5 82.2 0.43 3.0 1000 0.43 3.0 92
Mel4.0 73.1 0.58 4.0 82.2 0.43 3.0 1000 0.43 3.0 94
Mel4.5 82.3 0.65 4.5 82.2 0.43 3.0 1000 0.43 3.0 92
Mel5.0 91.4 0.70 5.0 82.2 0.43 3.0 1000 0.43 3.0 90