Table 1.
Drying Time of HAD Stage (h) | Drying Schemes | |||||||
---|---|---|---|---|---|---|---|---|
FD11-HAD | FD12-HAD | FD13-HAD | FD14-HAD | |||||
Tg (°C) | Tw (°C) | Tg (°C) | Tw (°C) | Tg (°C) | Tw (°C) | Tg (°C) | Tw (°C) | |
0 | −62.57 ± 2.21 i | −13 ± 2 h | −60.79 ± 2.67 f | −8 ± 1 g | −41.68 ± 2.10 e | −3 ± 1 e | −16.97 ± 1.29 d | 2 ± 1 d |
0.5 | −59.98 ± 2.27 h | 28 ± 2 g | −38.97 ± 2.19 e | 31 ± 2 f | −12.87 ± 1.79 d | 30 ± 2 d | 33.1 ± 1.65 c | 40 ± 1 c |
1.0 | −40.67 ± 2.17 g | 33 ± 1 f | −10.11 ± 1.96 d | 35 ± 1 e | 21.98 ± 1.98 c | 35 ± 2 c | 48.39 ± 1.43 b | 44 ± 1 b |
1.5 | −20.14 ± 1.28 f | 35 ± 1 e | 17.98 ± 1.08 c | 39 ± 1 d | 47.66 ± 1.87 b | 44 ± 1 b | 51.69 ± 1.65 a | 46 ± 1 a |
2.0 | 7.33 ± 1.01 e | 38 ± 1 d | 35.07 ± 1.41 b | 42 ± 1 c | 51.36 ± 1.70 a | 46 ± 1 a | 51.01 ± 1.57 a | 47 ± 1 a |
2.5 | 20.21 ± 1.01 d | 40 ± 1 c | 49.36 ± 1.89 a | 44 ± 1 b | 52.07 ± 1.60 a | 47 ± 1 a | ||
3.0 | 34.98 ± 1.54 c | 43 ± 1 b | 51.97 ± 1.76 a | 46 ± 1 a | ||||
3.5 | 48.39 ± 1.65 b | 45 ± 1 ab | 52.68 ± 1.89 a | 47 ± 1 a | ||||
4.0 | 51.01 ± 1.39 a | 46 ± 1 a | ||||||
4.5 | 52.07 ± 1.47 a | 47 ± 1 a | ||||||
5.0 | 52.14 ± 1.69 a | 47 ± 1 a |
Notes: Tg and Tw are the glass transition temperature and actual temperature of the sample center, respectively. Different letters indicate significant differences between different drying methods at different times (p < 0.05).