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1H-13C HSQC superimposition of TSP in black hydrolysed with cellulase and S-TSP_1 hydrolysed with xyloglucanase and cellulase in blue. Circled signals are related to sulphation. Galactose anomeric signals, α and β, are reported in the figure. The superscript corresponds to the carbon number of the observed monosaccharide, which is in bold, while the monosaccharide linked is in the parentheses. * signals assigned to the cellulose enzyme; Gal—galactose.
