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. Author manuscript; available in PMC: 2024 Dec 16.
Published in final edited form as: J Am Chem Soc. 2024 Apr 19;146(17):11616–11621. doi: 10.1021/jacs.4c03411

Table 2.

Nitrooxylation of HMB with Mn(NO3)3 Complexesa

Entry Complex % yield
1 2 99
2 4 b 58
3 2 (1 equiv) 50
4 2 (crude) 82
a

Conditions shown in Scheme 4.

b

24 h. Average yields for duplicated runs determined by 1H NMR.