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. 2024 Dec 16;14:30477. doi: 10.1038/s41598-024-79518-5

Table 2.

Application of the proposed TLC densitometric method for the determination of Migranil® tablets.

Taken µg/band Found ± SD* Pure added µg/band Found %**

MARGINAL Tablets

Batch No. t095003

Containing1 mg ergotamine tartarate, 10 mg phenobarbital sodium, 50 mg caffeine, 150 mg meprobamate, 200 mg dipyrone

ERG 0.10 102.04 ± 1.55 0.08 101.50
0.10 103.80
0.12 100.83
Mean ± SD 102.04 ± 1.56
PHEN 1.00 100.73 ± 1.80 0.80 100.16
1.00 99.30
1.20 102.75
Mean ± SD 100.74 ± 1.80
CAF 1.00 100.65 ± 0.92 0.80 101.12
1.00 99.60
1.20 101.25
Mean ± SD 100.66 ± 0.917
DIP 4.00 99.91 ± 1.781 3.20 99.46
4.00 101.87
4.80 98.39
Mean ± SD 99.91 ± 1.78
MEP 15.00 101.77 ± 1.299 12.00 103.17
15.00 100.60
18.00 101.55
Mean ± SD 101.77 ± 1.30

*Average of 6 determinations.

**Average of 3 determinations.