Table 1. Crystallographic data.
| Crystal | λ, Å | res., Å | I/σI* | Rm,† % | Multipl.‡ | Compl.,§ % |
|---|---|---|---|---|---|---|
| P. dejongeii BtubA-trx | ||||||
| space group P321, a = b = 180.5 Å, c = 84.2 Å | ||||||
| PEAK (Se) | 0.9793 | 3.1 | 19.7 (5.1) | 0.076 (0.332) | 8.3 | 99.9 (100.0) |
| INFL (Se) | 0.9796 | 3.1 | 20.3 (5.0) | 0.072 (0.347) | 8.4 | 99.9 (100.0) |
| HREM (Se) | 0.9184 | 3.1 | 19.0 (4.4) | 0.078 (0.392) | 8.2 | 99.9 (100.0) |
| NATI | 0.9340 | 2.5 | 12.5 (3.0) | 0.083 (0.452) | 4.9 | 99.9 (100.0) |
| P. dejongeii BtubA/B heterodimer | ||||||
| space group P6522, a = b = 154.4 Å, c = 256.3 Å | ||||||
| PEAK (Se) | 0.9790 | 4.0 | 11.4 (4.0) | 0.157 (0.429) | 8.1 | 99.7 (100.0) |
| NATI | 0.9340 | 3.2 | 12.8 (2.6) | 0.090 (0.379) | 3.6 | 99.0 (99.5) |
*
Signal-to-noise ratio of merged intensities; values in parentheses are for the highest resolution shell.
†
were I(h, i) are symmetry-related in tensities and I(h) is the mean intensity of the reflection with unique index h. The highest resolution bin is in parentheses.
‡
Multiplicity for unique (anomalously unique where appropriate) reflections.
§
Completeness for unique reflections; anomalous completeness is identical because inverse beam geometry was used. Values in parentheses are for the highest resolution bin. Correlation coefficients of anomalous differences at different wavelengths for the MAD experiment (cut at 4 Å): PEAK vs. INFL, 0.51; PEAK vs. HREM, 0.64; and INFL vs. HREM, 0.40.