Skip to main content
. 2024 Nov 30;22(12):539. doi: 10.3390/md22120539

Table 4.

1H and 13C NMR spectroscopic data of N-acetyl-6-dimethylallyl-l-tryptophan (4) in CD3OD-d4.

N-Acetyl-6-dimethylallyl-l-tryptophan (4) c
Position δC, Type δH, Mult
(J in Hz)
2 123.8, CH 7.01, s
3 110.9, C 4.70, dd (8.0, 5.0)
3a 127.1, C 3.31, m
4 119.0, CH 7.44, d (8.0)
5 120.9, CH 6.85, d (8.0)
6 136.3, C -
7 111.4, CH 7.11, s
7a 138.5, C -
8 28.6, CH2 3.31, m
3.12, dd (15.0, 8.0)
9 54.8, CH 4.70, dd (8.0, 5.0)
10 175.3, C -
11 173.2, C -
12 22.4, CH3 1.90, s
1′ 123.8, CH 7.01, s
2′ 173.2, C -
3′ 22.4, CH3 1.90, s
4′ 35.5, CH2 3.40, d (7.5)
5′ 125.6, CH 5.36, t (7.5)

c 1H and 13C NMR data were recorded at 900 and 225 MHz.