Table 4.
N-Acetyl-6-dimethylallyl-l-tryptophan (4) c | ||
---|---|---|
Position | δC, Type | δH, Mult (J in Hz) |
2 | 123.8, CH | 7.01, s |
3 | 110.9, C | 4.70, dd (8.0, 5.0) |
3a | 127.1, C | 3.31, m |
4 | 119.0, CH | 7.44, d (8.0) |
5 | 120.9, CH | 6.85, d (8.0) |
6 | 136.3, C | - |
7 | 111.4, CH | 7.11, s |
7a | 138.5, C | - |
8 | 28.6, CH2 | 3.31, m |
3.12, dd (15.0, 8.0) | ||
9 | 54.8, CH | 4.70, dd (8.0, 5.0) |
10 | 175.3, C | - |
11 | 173.2, C | - |
12 | 22.4, CH3 | 1.90, s |
1′ | 123.8, CH | 7.01, s |
2′ | 173.2, C | - |
3′ | 22.4, CH3 | 1.90, s |
4′ | 35.5, CH2 | 3.40, d (7.5) |
5′ | 125.6, CH | 5.36, t (7.5) |
c 1H and 13C NMR data were recorded at 900 and 225 MHz.