| Crystal data |
| Chemical formula |
(C2H7IN)2[GeI4] |
|
M
r
|
924.16 |
| Crystal system, space group |
Monoclinic, P21/n
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
8.1431 (2), 8.8362 (2), 25.1787 (7) |
| β (°) |
97.264 (2) |
|
V (Å3) |
1797.16 (8) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
11.99 |
| Crystal size (mm) |
0.14 × 0.08 × 0.01 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Analytical (CrysAlis PRO; Rigaku OD, 2023 ▸) |
|
Tmin, Tmax
|
0.399, 0.852 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
5413, 5413, 4967 |
|
R
int
|
0.030 |
| (sin θ/λ)max (Å−1) |
0.708 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.035, 0.092, 1.19 |
| No. of reflections |
5413 |
| No. of parameters |
121 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.21, −1.27 |
