| Crystal data |
| Chemical formula |
C30H23NO2
|
|
M
r
|
429.49 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
9.6337 (1), 9.8825 (2), 12.8446 (3) |
| α, β, γ (°) |
87.546 (2), 86.605 (1), 70.914 (3) |
|
V (Å3) |
1153.26 (4) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.08 |
| Crystal size (mm) |
0.29 × 0.24 × 0.20 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE diffractometer with PHOTON II detector |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.786, 0.841 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
17043, 4720, 3564 |
|
R
int
|
0.027 |
| (sin θ/λ)max (Å−1) |
0.627 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.042, 0.120, 1.03 |
| No. of reflections |
4720 |
| No. of parameters |
353 |
| No. of restraints |
186 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.14, −0.18 |
