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. 2025 Feb 3;14(2):207–213. doi: 10.1021/acsmacrolett.4c00839

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© 2025 The Authors. Published by American Chemical Society

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(A) Reaction scheme of ATRP grafting-from BB synthesis using various (meth-)acrylate monomers. (B) SEC trace of P(LABiB-co-BiBOEA)₁₄₀ macroinitiator overlaid with corresponding traces of PBA and PTEGA BB after ATRP grafting-from. (C) PTEGA BB polymers of varying backbone lengths (DP_bb). (D) SEC traces showing degradation of PBA BB using 0.5 M dithiothreitol (DTT) in DMF at 22 °C, after 24 h. (E) SEC traces showing degradation of PTEGA BB using 0.1 M tris(2-carboxyethyl) phosphine (TCEP) in water at 22 °C, after 24 h.