Table 5. Intramolecular and Intermolecular Competition Studies on the Effect of Base in Amidation reactionsa.
| entry | base | 4b (%) | 2a (%) | 6b (%) | unknown (%) |
|---|---|---|---|---|---|
| 1 | triethylamine | 23 | 8 | 3 | 2 |
| 2 | 2,6-lutidine | 44 | 5 | 0 | 0 |
Yield was determined with 19F{1H}-NMR using α,α,α-trifluorotoluene as an internal standard.
