Table 2. 13C NMR Data (150 MHz, DMSO-d6) of Compounds 1–8a.
| Position | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 |
|---|---|---|---|---|---|---|---|---|
| 1 | 59.5, CH2 | 59.5, CH2 | 59.4, CH2 | 59.4, CH2 | 59.4, CH2 | 59.4, CH2 | 59.0, CH2 | 59.5, CH2 |
| 2 | 44.4, CH2 | 44.4, CH2 | 44.4, CH2 | 44.4, CH2 | 44.4, CH2 | 44.4, CH2 | 42.6, CH2 | 44.4, CH2 |
| 4 | 65.2, CH | 65.2, CH | 65.2, CH | 65.3, CH | 65.2, CH | 65.2, CH | 97.2, C | 65.2, CH |
| 5 | 44.3, CH2 | 44.3, CH2 | 44.2, CH2 | 44.3, CH2 | 44.2, CH2 | 44.3, CH2 | 52.8, CH2 | 44.3, CH2 |
| 6 | 81.0, C | 81.0, C | 81.0, C | 81.0, C | 81.0, C | 81.0, C | 78.9, C | 81.0, C |
| 7 | 43.1, CH | 43.1, CH | 43.0, CH | 43.1, CH | 43.0, CH | 43.2, CH | 46.7, CH | 43.1, CH |
| 8 | 163.3, C | 163.4, C | 163.2, C | 163.3, C | 163.3, C | 163.3, C | 56.6, CH | 163.4, C |
| 9 | 126.9, C | 126.9, C | 126.8, C | 126.9, C | 126.9, C | 127.4, C | 42.1, CH | 126.9, C |
| 10 | 173.8, C | 173.8, C | 173.9, C | 173.9, C | 173.8, C | 173.8, C | 175.2, C | 173.8, C |
| 11 | 19.9, CH2 | 20.0, CH2 | 19.9, CH2 | 19.9, CH2 | 19.9, CH2 | 20.1, CH2 | 26.0, CH2 | 20.0, CH2 |
| 12 | 25.5, CH2 | 25.4, CH2 | 25.6, CH2 | 25.5, CH2 | 25.5, CH2 | 25.1, CH2 | 25.5, CH2 | 25.4, CH2 |
| 13 | 45.3, CH | 45.2, CH | 45.4, CH | 45.3, CH | 45.3, CH | 45.1, CH | 42.5, CH | 45.2, CH |
| 14 | 46.6, CH | 46.8, CH | 46.6, CH | 46.9, CH | 46.8, CH | 48.6, CH | 49.9, CH | 46.8, CH |
| 15 | 25.8, CH2 | 25.9, CH2 | 25.6, CH2 | 25.8, CH2 | 25.7, CH2 | 28.6, CH2 | 26.8, CH2 | 25.9, CH2 |
| 16 | 43.4, CH2 | 43.5, CH2 | 43.5, CH2 | 43.4, CH2 | 43.4, CH2 | 43.3, CH2 | 45.4, CH2 | 43.5, CH2 |
| 17 | 43.5, C | 43.5, C | 40.1, C | 43.5, C | 43.5, C | 43.6, C | 42.9, C | 43.5, C |
| 18 | 42.1, CH2 | 42.1, CH2 | 42.1, CH2 | 42.1, CH2 | 42.1, CH2 | 41.8, CH2 | 44.9, CH2 | 42.1, CH2 |
| 19 | 27.2, CH3 | 27.2, CH3 | 27.2, CH3 | 27.2, CH3 | 27.2, CH3 | 27.2, CH3 | 25.5, CH3 | 27.2, CH3 |
| 20 | 21.0, CH3 | 21.0, CH3 | 20.9, CH3 | 21.0, CH3 | 20.9, CH3 | 21.3, CH3 | 22.4, CH3 | 21.0, CH3 |
| 21 | 32.7, CH | 32.6, CH | 32.8, CH | 32.9, CH | 32.9, CH | 34.1, CH | 31.3, CH | 32.5, CH |
| 22 | 35.7, CH2 | 37.0, CH2 | 36.9, CH2 | 37.3, CH2 | 37.1, CH2 | 137.0, CH | 37.7, CH2 | 37.1, CH2 |
| 23 | 26.1, CH2 | 25.0, CH2 | 24.8, CH2 | 24.5, CH2 | 24.2, CH2 | 122.2, CH | 25.52, CH2 | 25.5, CH2 |
| 24 | 140.7, CH | 123.4, CH | 33.8, CH2 | 33.2, CH2 | 32.9, CH2 | 120.4, CH | 124.6, CH | 124.5, CH |
| 25 | 128.3, C | 135.4, C | 39.3, CH | 35.4, CH | 32.0, CH | 134.8, C | 130.6, C | 130.7, C |
| 26 | 169.2, C | 66.4, CH2 | 165.5, C | 66.3, CH2 | 67.9, CH2 | 26.2, CH3 | 25.5, CH3 | 25.5, CH3 |
| 27 | 17.1, CH3 | 17.3, CH3 | 17.2, CH3 | 17.3, CH3 | 17.3, CH3 | 20.6, CH3 | 18.2, CH3 | 17.3, CH3 |
| 28 | 12.3, CH3 | 13.5, CH3 | 17.2, CH3 | 16.8, CH3 | 16.5, CH3 | 18.0, CH3 | 17.5, CH3 | 17.5, CH3 |
| 29 | 162.2, CH |
δC in ppm.