Table 2.
13C NMR data (CD3CN, 150 MHz) for bulbillosins A–E (1–5).
| Position | 1 | 2 | 3 | 4 | 5 |
|---|---|---|---|---|---|
| 1 | 145.5 | 154.3 | 154.5 | 145.7 | 145.6 |
| 3 | 154.9 | 155.1 | 156.3 | 155.9 | 155.0 |
| 4 | 111.9 | 113.6 | 112.9 | 112.1 | 111.8 |
| 4a | 146.1 | 145.0 | 145.6 | 147.2 | 147.7 |
| 5 | 106.8 | 106.1 | 105.9 | 106.7 | 105.5 |
| 6 | 192.7 | 191.3 | 191.7 | 192.8 | 199.4 |
| 7 | 83.6 | 88.9 | 88.9 | 84.1 | 74.5 |
| 8 | 45.2 | 166.0 | 166.3 | 45.4 | 41.7 |
| 8a | 116.7 | 112.8 | 112.3 | 116.9 | 121.3 |
| 9 | 19.1 | 26.1 | 26.2 | 19.2 | 21.3 |
| 10 | 131.0 | 130.2 | 120.3 | 120.9 | 131.5 |
| 11 | 162.4 | 164.0 | 139.9 | 139.9 | 162.4 |
| 12 | 41.4 | 41.5 | 122.6 | 122.5 | 41.4 |
| 13 | 65.3 | 65.5 | 132.4 | 132.1 | 65.6 |
| 14 | 46.6 | 46.6 | 114.3 | 114.3 | 46.7 |
| 15 | 195.5 | 194.8 | 156.3 | 155.9 | 194.7 |
| 16 | 22.8 | 22.9 | 19.8 | 19.7 | 22.8 |
| 17 | 171.5 | 168.9 | 166.3 | 171.8 | - |
| 18 | 51.6 | 125.9 | 129.4 | 51.6 | 36.8 |
| 19 | 192.3 | 185.9 | 185.7 | 192.2 | 203.5 |
| 20 | 128.1 | 127.0 | 127.0 | 128.0 | 129.2 |
| 21 | 147.2 | 146.5 | 146.5 | 147.2 | 143.4 |
| 22 | 129.4 | 129.3 | 129.4 | 129.2 | 129.2 |
| 23 | 145.4 | 145.5 | 145.4 | 145.8 | 144.4 |
| 24 | 129.5 | 129.3 | 129.3 | 129.2 | 129.2 |
| 25 | 149.3 | 149.0 | 149.0 | 149.0 | 147.7 |
| 26 | 35.7 | 35.7 | 35.6 | 35.6 | 35.6 |
| 27 | 44.6 | 44.5 | 44.5 | 44.6 | 44.7 |
| 28 | 32.9 | 32.8 | 32.7 | 32.8 | 32.6 |
| 29 | 30.5 | 30.5 | 30.4 | 30.6 | 30.5 |
| 30 | 11.4 | 11.4 | 11.4 | 11.5 | 11.4 |
| 31 | 19.2 | 19.2 | 19.2 | 19.2 | 19.3 |
| 32 | 21.3 | 21.2 | 21.2 | 21.3 | 21.3 |