. 2025 Feb 20;10(8):8729–8735. doi: 10.1021/acsomega.5c00337

Table 3. ¹H NMR Results of a Sample of 2 mL of 18.7 mM NH₄Cl, 40 μL of 1M H₂SO₄, and 200 μL of DMSO-d₆ with Different Pulse Sequences and bi-Waltz65-256pl Decoupling by Using a 10 mm BBO Probe.

NMR tube size	pluse sequence	decoupling method	S/N	S/N gain
10 mm	zgesgp	No	3347
10 mm	zgesgpig	bi-Waltz65–256pl	8974	2.7
10 mm	zgesfpgpig	bi-Waltz65–256pl	10,831	3.2

Table 3. 1H NMR Results of a Sample of 2 mL of 18.7 mM NH4Cl, 40 μL of 1M H2SO4, and 200 μL of DMSO-d6 with Different Pulse Sequences and bi-Waltz65-256pl Decoupling by Using a 10 mm BBO Probe.