Table 5.
Carbon atoms of DH alone and their chemical shifts in mixtures of P4, P5, and P7.
Position of P1 Protons | Chemical Shifts of P1 | Chemical Shifts of P5 | Chemical Shifts of P4 | Chemical Shifts of P7 |
---|---|---|---|---|
C1 | 211.33 | 207.80 | 211.66 | 207.85 |
C6 | 155.38 | 155.75 | 155.48 | 155.74 |
C8 | 151.38 | - | 151.52 | - |
C5 | 148.15 | 148.92 | 148.24 | 148.91 |
C18 | 130.69 | 130.70 | 130.77 | 130.72 |
C19 | 129.67 | 129.80 | 129.73 | 129.83 |
C20 | 128.79 | 128.87 | 128.83 | 128.88 |
C17 | 128.42 | 128.13 | 128.39 | 128.10 |
C9 | 127.24 | 127.55 | 127.43 | 127.55 |
C7 | 107.48 | 107.02 | 107.65 | 107.05 |
C4 | 105.41 | 103.97 | 103.68 | 103.96 |
C10 | 55.79 | 55.94 | 55.69 | 55.94 |
C11 | 55.24 | 55.77 | 55.29 | 55.76 |
C2 | 44.82 | 43.90 | 44.68 | 43.91 |
C3 | 32.42 | 31.56 | 31.01 | 31.55 |
C15 | 52.21 | 51.75 | 52.10 | 51.76 |
C12 | 36.63 | 37.48 | 36.57 | 37.55 |
C14 | 29.58 | 29.29 | 29.32 | 29.44 |
C14′ | 28.24 | 28.22 | 28.11 | 28.09 |
C16 | 60.63 | Overlappted peak | 60.17 | Overlappted peak |