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N-phenyl-5-(p-tolyl)-6H-1,3,4-thiadiazin-2-amine—IJ29 Yellow solid; yield 50%; mp 180–181 °C; HPLC-UV: 3.18 min.; purity of 99%; 1H NMR (600 MHz, DMSO-d6) δ 2.39 (s, 3H, CH3); 4.29 (s, 2H, CH2); 7.35–7.38 (m, 3H, H-Ar); 7.42–7.43 (m, 2H, H-Ar); 7.50 (t, 2H, J = 8.09 Hz, H-Ar); 7.84 (d, 2H, J = 8.3 Hz, H-Ar); 13C NMR (150 MHz, DMSO-d6) δ 142.3; 130.6; 130.1; 130.0; 129.2; 127.7; 127.6; 124.8; 123.9; 23.1; 21.5. 13C NMR (150 MHz, DMSO-d6) δ 159.3; 147.2; 129.1; 128.2; 126.4; 123.1; 122.0; 116.5; 115.9; 115.5; 22.6. |
IJ 29 |
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