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. 2025 Mar 11;81(Pt 4):303–309. doi: 10.1107/S2056989025002063

Table 2. Selected bond lengths (Å), angles (°) and torsion angles (°) of the Hbtc2− anion in 1.

C1—C6 1.393 (2) C2—C3 1.39 (2) C4—C5 1.392 (2)
C1—C2 1.398 (2) C3—C4 1.391 (2) C5—C6 1.388 (2)
C2—C19 1.504 (2) C4—C18 1.486 (2) C6—C17 1.510 (2)
O7—C17 1.255 (2) O9—C18 1.214 (2) O11—C19 1.2555 (19)
O8—C17 1.2650 (19) O10—C18 1.338 (2) O12—C19 1.263 (2)
C2—C3—C4 119.79 (15) C6—C1—C2 120.38 (16) O7—C17—O8 125.41 (15)
C6—C5—C4 120.39 (15) C3—C2—C1 119.79 (14) O9—C18—O10 123.24 (16)
C3—C4—C5 120.21 (16) C5—C6—C1 119.38 (15) O11—C19—O12 124.16 (15)
C1—C6—C17—O7 15.5 (2) C3—C4—C18—O10 17.1 (2) C1—C2—C3—C4 2.5 (2)
C5—C6—C17—O7 167.31 (14) C5—C4—C18—O10 164.63 (14) C2—C3—C4—C5 −0.5 (2)
C1—C6—C17—O8 163.84 (15) C1—C2—C19—O11 −163.18 (15) C2—C1—C6—C5 −0.4 (2)
C5—C6—C17—O8 −13.4 (2) C3—C2—C19—O11 13.5 (2) C3—C4—C5—C6 −1.5 (2)
C3—C4—C18—O9 −163.64 (16) C1—C2—C19—O12 15.8 (2) C4—C5—C6—C1 1.6 (2)
C5—C4—C18—O9 14.6 (2) C3—C2—C19—O12 −167.44 (15) C6—C1—C2—C3 −2.4 (2)