1. Average Crystallite Size ⟨D XRD⟩; Average Particle Diameter ⟨D TEM⟩, Polydispersity (PD), Hydrodynamic Diameter (d H), and Polydispersity Indices (PDI) .
| sample | ⟨D XRD⟩ (nm) | ⟨D TEM⟩ (nm) | PD (nm–1) | dH (nm) | PDI |
|---|---|---|---|---|---|
| FO | 5.5(6) | 5.1(5) | 9.8(1) | - | - |
| FOdm | - | 5.5(9) | 16.3(1) | 42.8 (4) | 0.37 |
| FOim | - | 5.7(9) | 15.7(1) | 40.5 (4) | 0.37 |
| CZFO | 5.2(5) | 5.0(1) | 2.0(1) | - | - |
| CZFOdm | - | 5.3(5) | 16.9(1) | 14.3(2) | 0.37 |
| CZFOim | - | 5.1(5) | 9.8(1) | 18.3(2) | 0.37 |
| CFO | 4.9(5) | 4.6(4) | 8.6(1) | - | - |
| CFOdm | - | 4.8(5) | 10.4(1) | 29.3(3) | 0.39 |
| CFOim | - | 5.1(5) | 9.8(1) | 34.3(3) | 0.40 |
a
Uncertainties in the last digit are given in parentheses.