2. Proposed Species after Each Decomposition Step upon Heating.
| mass
loss |
|||
|---|---|---|---|
| decomposition step and temperature | actual (%) | theoretical (%) | primary species present at end of decomposition step |
| 1 (<200 °C) | 14.51 | N/A | neodymium citrate, residual organics (e.g., HMTA, urea) |
| 2 (∼225 °C) | 22.95 | N/A | neodymium citrate, residual HMTA and urea decomposition products |
| 3 (∼320 °C) | 25.06 | N/A | neodymium aconitate (possibly some residual neodymium citrate) |
| 4 (∼420 °C) and 5 (∼550 °C) | 9.30 | 9.34 | neodymium carbonate |
| 6 (>570 °C) | 7.01 | 7.90 | neodymium oxide |