| Crystal data |
| Chemical formula |
[Cd(NO3)2(C7H6N2O)4] |
|
M
r
|
772.97 |
| Crystal system, space group |
Monoclinic, C2/c
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
15.9012 (3), 11.0897 (2), 18.9475 (5) |
| β (°) |
109.182 (3) |
|
V (Å3) |
3155.70 (13) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
6.19 |
| Crystal size (mm) |
0.10 × 0.08 × 0.06 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Single source at home/near, HyPix3000 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2020 ▸) |
|
Tmin, Tmax
|
0.016, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
12616, 3014, 2324 |
|
R
int
|
0.084 |
| (sin θ/λ)max (Å−1) |
0.614 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.049, 0.128, 1.01 |
| No. of reflections |
3014 |
| No. of parameters |
223 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.56, −0.95 |
