Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C29H22F3NO7S |
| M r | 585.53 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 7.6375 (5), 11.0324 (6), 30.2019 (8) |
| β (°) | 93.983 (1) |
| V (Å3) | 2538.7 (2) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 1.79 |
| Crystal size (mm) | 0.35 × 0.18 × 0.17 |
| Data collection | |
| Diffractometer | Rigaku XtaLAB Synergy-S, HyPix-6000HE area-detector |
| Absorption correction | Multi-scan (CrysAlis PRO; Rigaku OD, 2021 ▸) |
| Tmin, Tmax | 0.713, 0.737 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 31570, 5526, 5187 |
| R int | 0.049 |
| (sin θ/λ)max (Å−1) | 0.639 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.037, 0.103, 1.05 |
| No. of reflections | 5526 |
| No. of parameters | 379 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.45, −0.43 |