| Bruker D8 QUEST PHOTON 3 diffractometer | 3139 independent reflections |
| Radiation source: INCOATEC IµS micro—-focus source | 2827 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.077 |
| Detector resolution: 7.3910 pixels mm-1 | θmax = 72.4°, θmin = 5.3° |
| φ and ω scans | h = −10→9 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −17→17 |
| Tmin = 0.77, Tmax = 0.88 | l = −16→16 |
| 33748 measured reflections |