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. 2025 May 20;81(Pt 6):534–537. doi: 10.1107/S2056989025004293

Table 1. Experimental details.

Crystal data
Chemical formula [Ni(C18H18S2)2]
M r 655.60
Crystal system, space group Monoclinic, P21/c
Temperature (K) 150
a, b, c (Å) 8.4446 (2), 14.0911 (2), 13.5880 (2)
β (°) 96.133 (1)
V3) 1607.63 (5)
Z 2
Radiation type Cu Kα
μ (mm−1) 3.47
Crystal size (mm) 0.14 × 0.14 × 0.04
 
Data collection
Diffractometer Bruker D8 QUEST PHOTON 3 diffractometer
Absorption correction Multi-scan (SADABS; Krause et al., 2015)
Tmin, Tmax 0.77, 0.88
No. of measured, independent and observed [I > 2σ(I)] reflections 33748, 3139, 2827
R int 0.077
(sin θ/λ)max−1) 0.618
 
Refinement
R[F2 > 2σ(F2)], wR(F2), S 0.024, 0.066, 1.08
No. of reflections 3139
No. of parameters 191
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.29, −0.30

Computer programs: APEX4 and SAINT (Bruker, 2021), SHELXT (Sheldrick, 2015a), SHELXL2018/1 (Sheldrick, 2015b) and SHELXTL (Sheldrick, 2008).