Table 1. Experimental details.
| Crystal data | |
| Chemical formula | [Ni(C18H18S2)2] |
| M r | 655.60 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 150 |
| a, b, c (Å) | 8.4446 (2), 14.0911 (2), 13.5880 (2) |
| β (°) | 96.133 (1) |
| V (Å3) | 1607.63 (5) |
| Z | 2 |
| Radiation type | Cu Kα |
| μ (mm−1) | 3.47 |
| Crystal size (mm) | 0.14 × 0.14 × 0.04 |
| Data collection | |
| Diffractometer | Bruker D8 QUEST PHOTON 3 diffractometer |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.77, 0.88 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 33748, 3139, 2827 |
| R int | 0.077 |
| (sin θ/λ)max (Å−1) | 0.618 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.024, 0.066, 1.08 |
| No. of reflections | 3139 |
| No. of parameters | 191 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.29, −0.30 |