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. 2025 Jun 18;15(26):20623–20628. doi: 10.1039/d5ra01979f

Table 2. Investigation of the catalyst loading effect on the synthesis of compound 3aa.

Entry Amount of the catalyst system Yieldb (%)
1 FeCl3·6H2O (5 mol%) 78
2 FeCl 3 ·6H 2 O (10 mol%) 84
3 FeCl3·6H2O (15 mol%) 84
a

Reaction conditions: methyl arene 1a (1.0 mmol), acetophenone 2a (1.0 mmol), and iron as the catalyst 3a (10 mmol).

b

Isolated yields.