2. Binding Constant Values (K ass, M–1) Determined by NMR Experiments (SI) and Chiral Selectivity Ratio Calculated by HR-MS Spectrometry Experiments.
| guest | Kass G+@ PrS[4] iPe | chiral selectivity R L/R D |
|---|---|---|
| 6 2+ | 1900 | 2.01 |
| 7 + | 40,000 | 1.22 |
| 8 + | 290 | 0.94 |
| 9 + | 690 | 0.70 |
Calculated by integrating the free and complexed 1H NMR signals of the host.
Calculated using a 1H NMR competition experiment with methoxy-prism[5]arene as a competitive host.