Table 1.
Data collection and refinement statistics (molecular replacement)
| hRpn13:ENT complex | |
|---|---|
| Data collection | |
| Space group | P212121 |
| Cell dimensions | |
| a, b, c (Å) | 31.26, 56.97, 77.79 |
| α, β, γ (°) | 90, 90, 90 |
| Resolution (Å) | 38.9-1.85 (1.916 – 1.85) a |
| Rsym or Rmerge | 0.07717 (0.2239) |
| I / σI | 12.49 (6.97) |
| Completeness (%) | 99.27 (99.83) |
| Redundancy | 6.4 (6.7) |
| Refinement | |
| Resolution (Å) | 1.85 |
| No. reflections | 79094 (8084) |
| Rwork / Rfree | 0.1951/0.2160 |
| No. atoms | |
| Protein | 968 |
| Ligand/ion | 8 |
| Water | 61 |
| B-factors | |
| Protein | 17.76 |
| Ligand/ion | 26.23 |
| Water | 25.56 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.011 |
| Bond angles (°) | 1.31 |
aValues in parentheses are for the high-resolution shell.