| Crystal data |
| Chemical formula |
[Pd(C5H5NO2)(C28H38N2O2P2)]·0.5C7H8
|
|
M
r
|
760.11 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
9.5548 (2), 10.7020 (3), 18.4654 (5) |
| α, β, γ (°) |
74.0508 (10), 86.9998 (10), 76.0888 (9) |
|
V (Å3) |
1762.06 (8) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
5.45 |
| Crystal size (mm) |
0.19 × 0.08 × 0.03 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.42, 0.85 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
27460, 6223, 5975 |
|
R
int
|
0.030 |
| (sin θ/λ)max (Å−1) |
0.596 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.022, 0.057, 1.06 |
| No. of reflections |
6223 |
| No. of parameters |
456 |
| No. of restraints |
43 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.38, −0.32 |
