| Oxford Diffraction Xcalibur, Eos diffractometer | 3172 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2592 reflections with I > 2σ(I) |
| Detector resolution: 16.1419 pixels mm-1 | Rint = 0.078 |
| ω scan | θmax = 30.0°, θmin = 2.2° |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2013) | h = −17→17 |
| Tmin = 0.471, Tmax = 1.000 | k = −26→26 |
| 30092 measured reflections | l = −13→13 |
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