Table 9. Hydrogen-bond geometry (Å, °) for 2c.
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N11—H01⋯Cl21 | 0.90 (2) | 2.18 (3) | 3.073 (5) | 171 (5) |
| N11—H02⋯Cl6i | 0.89 (2) | 2.60 (5) | 3.335 (5) | 140 (6) |
| N21—H03⋯Cl21 | 0.90 (2) | 2.30 (2) | 3.182 (5) | 167 (4) |
| N21—H04⋯Cl22 | 0.90 (2) | 2.50 (4) | 3.252 (5) | 142 (4) |
| N31—H05⋯Cl21 | 0.90 (2) | 2.22 (3) | 3.099 (5) | 167 (6) |
| N31—H06⋯Cl22 | 0.90 (2) | 2.27 (3) | 3.134 (5) | 162 (7) |
| N41—H07⋯Cl23 | 0.89 (2) | 2.32 (2) | 3.196 (5) | 171 (5) |
| N41—H08⋯Cl22 | 0.89 (2) | 2.59 (6) | 3.224 (5) | 129 (6) |
| N51—H09⋯Cl22 | 0.93 (3) | 2.33 (4) | 3.180 (5) | 151 (6) |
| N51—H010⋯Cl23 | 0.93 (3) | 2.22 (3) | 3.126 (5) | 166 (6) |
| N61—H61B⋯Cl23 | 0.91 | 2.28 | 3.161 (6) | 164 |
| N61—H61A⋯Cl24 | 0.91 | 2.57 | 3.325 (5) | 141 |
| N71—H71A⋯Cl23 | 0.91 | 2.32 | 3.216 (5) | 169 |
| N71—H71B⋯Cl24 | 0.91 | 2.57 | 3.254 (5) | 132 |
| N81—H81B⋯Cl25 | 0.91 | 2.26 | 3.157 (5) | 170 |
| N81—H81A⋯Cl24 | 0.91 | 2.24 | 3.146 (5) | 175 |
| N91—H017⋯Cl24 | 0.93 (3) | 2.56 (6) | 3.356 (5) | 144 (7) |
| N91—H018⋯Cl25 | 0.93 (3) | 2.23 (3) | 3.134 (5) | 163 (7) |
| N101—H019⋯Cl5 | 0.93 (3) | 2.64 (4) | 3.459 (5) | 147 (6) |
| N101—H019⋯Cl8 | 0.93 (3) | 2.72 (5) | 3.471 (5) | 138 (6) |
| N101—H020⋯Cl25 | 0.93 (3) | 2.15 (3) | 3.075 (5) | 170 (4) |
Symmetry code: (i)
.